Practical Instrumental Analysis : Methods, Quality Assurance and Laboratory Management
Sergio. Petrozzi
Bok Engelsk 2012 · Electronic books.
| Utgitt | Hoboken : : Wiley, , 2012.
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| Omfang | 1 online resource (493 p.)
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| Opplysninger | Description based upon print version of record.. - Title page; Copyright page; Contents; Preface to the German Edition; Preface to the English Edition; Dedication; Foreword; 1: Introduction; 1.1 Analytical Chemistry - The History; 1.2 Analytical Chemistry and Its Role in Today's Society; 2: Introduction to Quality Management; 2.1 Historical Background; 2.2 Variability; 2.3 The Four Pillars of Wisdom (from Shewhart to Deming); 2.4 Zero-Defect Tolerance; 2.5 Why Standards?; 2.6 The Controlled Process; 2.7 ISO Guidelines 9004; 2.8 Quality Management System (QMS) Requirements; 3: Fundamentals of Statistics; 3.1 Basic Concepts. - 3.1.1 Population and Sample3.1.2 Distribution of Values; 3.2 Important Terms; 3.2.1 Mean, Arithmetic Mean, Average ; 3.2.2 Standard Deviation (σ, s); 3.2.3 Variance (Var,V); 3.2.4 Standard Deviation of Mean Values ; 3.2.5 Relative Standard Deviation (RSD) and Coefficient of Variation (CV); 3.2.6 Confidence Interval (CI), Confidence Limits; 3.3 Quality of Results (Accuracy and Precision); 3.3.1 Measurement Deviations; 3.3.2 Random Deviations - Influence on Precision; 3.3.3 Systematic Deviations - Influence on Accuracy; 3.3.4 Gross Errors; 3.3.5 Uncertainty of Measurement Results. - 3.3.6 Non-statistical Methods of Estimation3.3.7 Expressing Analytical Results; 3.3.8 Significant Figures - "Box-and-Dot" Method; 3.3.9 Outlier Tests; 3.4 Regression; 3.4.1 Regression Analysis; 3.4.2 Calibration Function; 3.4.3 The "Optimal" Trend Line; 3.4.4 Linear Regression; 4: The Analytical Process; 4.1 The Analytical Process in the Overall Context; 4.2 Planning Phase; 4.2.1 Analytical Problem; 4.2.2 Object of Investigation; 4.2.3 Sample; 4.2.4 Sampling; 4.2.5 Examination Procedures; 4.2.6 Analyte; 4.2.7 Literature and Database Research; 4.3 Analysis; 4.3.1 Measurement. - 4.3.2 Method Optimization4.3.3 Calibration; 4.4 Assessment; 4.4.1 Quantification; 4.4.2 ("True") Content; 4.5 Validation; 4.5.1 Validation Elements; 4.5.2 Using the Computer; 4.6 Final Documentation; 4.6.1 Review; 5: Example of a Validation Strategy; 5.1 Determination of Phenol in Industrial Waste Water; 5.1.1 Confirmation of Identity; 5.1.2 Sample Content Determination; 5.1.3 Selection; 6: Organizational and Practical Procedures in the Teaching Laboratory Program; 6.1 Goals; 6.2 Safety in the Laboratory Class; 6.3 Experimental Project Workflow; 6.3.1 Preparation; 6.3.2 Laboratory Notebook. - 6.4 ReportsReferences; 7: Literature; 7.1 Cited Literature; 7.2 Recommended Norms (Selection); 7.2.1Calibration; 7.2.2Inter-laboratory Tests; 7.2.3Quality Management; 7.3 Suggested Books (Selection); 8: Projects; 8.1 Chromatography; 8.1.1 Gas Chromatography - GC, Project: Tanker Accident; 8.1.1.1 Analytical Problem; 8.1.1.2 Introduction; 8.1.1.3 Material and Methods; 8.1.1.4 Questions; References; 8.1.2 Gas Chromatography Coupled with Mass Selective Detection - GC/MS, Project: "Circumvention of the Formerly Mandatory Declaration of Fragrances in Perfumes?"; 8.1.2.1 Analytical Problem. - 8.1.2.2 Introduction. - This practical book in instrumental analytics conveys an overview of important methods of analysis and enables the reader to realistically learn the (principally technology-independent) working techniques the analytical chemist uses to develop methods and conduct validation.What is to be conveyed to the student is the fact that analysts in their capacity as problem-solvers perform services for certain groups of customers, i.e., the solution to the problem should in any case be processed in such a way as to be ""fit for purpose"".The book presents sixteen experiments
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| Emner | |
| Sjanger | |
| Dewey | |
| ISBN | 9783527329519
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